1H-13C CP 1, -3249, 30119.3298, 299.292247 2, -2203, 30114.4857, 299.244112 3, -1048, 30109.6417, 299.195978 4, -1004, 30104.7976, 299.147843 5, -1216, 30099.9536, 299.099708 6, 183, 30095.1095, 299.051573 7, 3700, 30090.2654, 299.003438 8, 7359, 30085.4214, 298.955303 9, 8268, 30080.5773, 298.907168 10, 5469, 30075.7333, 298.859034 11, 1215, 30070.8892, 298.810899 12, -822, 30066.0451, 298.762764 13, 1179, 30061.2011, 298.714629 14, 5545, 30056.3570, 298.666494 15, 8678, 30051.5130, 298.618359 16, 8293, 30046.6689, 298.570224 17, 5213, 30041.8248, 298.522090 18, 2168, 30036.9808, 298.473955 19, 1038, 30032.1367, 298.425820 20, 1393, 30027.2927, 298.377685 21, 1626, 30022.4486, 298.329550 22, 1173, 30017.6045, 298.281415 23, 1245, 30012.7605, 298.233280 24, 3262, 30007.9164, 298.185146 25, 6751, 30003.0724, 298.137011 26, 9164, 29998.2283, 298.088876 27, 8070, 29993.3842, 298.040741 28, 3606, 29988.5402, 297.992606 29, -1336, 29983.6961, 297.944471 30, -3505, 29978.8521, 297.896336 31, -2026, 29974.0080, 297.848202 32, 1113, 29969.1639, 297.800067 33, 3155, 29964.3199, 297.751932 34, 3129, 29959.4758, 297.703797 35, 2408, 29954.6318, 297.655662 36, 2930, 29949.7877, 297.607527 37, 4993, 29944.9436, 297.559392 38, 6831, 29940.0996, 297.511258 39, 6300, 29935.2555, 297.463123 40, 2983, 29930.4115, 297.414988 41, -1248, 29925.5674, 297.366853 42, -3640, 29920.7233, 297.318718 43, -2653, 29915.8793, 297.270583 44, 949, 29911.0352, 297.222448 45, 4673, 29906.1912, 297.174314 46, 5903, 29901.3471, 297.126179 47, 3411, 29896.5030, 297.078044 48, -2033, 29891.6590, 297.029909 49, -8124, 29886.8149, 296.981774 50, -12282, 29881.9709, 296.933639 51, -13058, 29877.1268, 296.885504 52, -10872, 29872.2827, 296.837370 53, -7511, 29867.4387, 296.789235 54, -4687, 29862.5946, 296.741100 55, -2812, 29857.7506, 296.692965 56, -1139, 29852.9065, 296.644830 57, 821, 29848.0624, 296.596695 58, 2087, 29843.2184, 296.548561 59, 737, 29838.3743, 296.500426 60, -3981, 29833.5303, 296.452291 61, -9981, 29828.6862, 296.404156 62, -13168, 29823.8421, 296.356021 63, -10590, 29818.9981, 296.307886 64, -3247, 29814.1540, 296.259751 65, 4246, 29809.3100, 296.211617 66, 7214, 29804.4659, 296.163482 67, 4705, 29799.6218, 296.115347 68, 75, 29794.7778, 296.067212 69, -2144, 29789.9337, 296.019077 70, -173, 29785.0897, 295.970942 71, 3922, 29780.2456, 295.922807 72, 6715, 29775.4015, 295.874673 73, 6784, 29770.5575, 295.826538 74, 5569, 29765.7134, 295.778403 75, 5126, 29760.8694, 295.730268 76, 5444, 29756.0253, 295.682133 77, 4371, 29751.1812, 295.633998 78, 264, 29746.3372, 295.585863 79, -5554, 29741.4931, 295.537729 80, -9416, 29736.6491, 295.489594 81, -8696, 29731.8050, 295.441459 82, -4576, 29726.9609, 295.393324 83, -1241, 29722.1169, 295.345189 84, -2011, 29717.2728, 295.297054 85, -6105, 29712.4288, 295.248919 86, -9215, 29707.5847, 295.200785 87, -7455, 29702.7406, 295.152650 88, -967, 29697.8966, 295.104515 89, 6145, 29693.0525, 295.056380 90, 9419, 29688.2085, 295.008245 91, 7792, 29683.3644, 294.960110 92, 4225, 29678.5203, 294.911975 93, 2927, 29673.6763, 294.863841 94, 5859, 29668.8322, 294.815706 95, 11408, 29663.9882, 294.767571 96, 15876, 29659.1441, 294.719436 97, 16108, 29654.3000, 294.671301 98, 11257, 29649.4560, 294.623166 99, 2928, 29644.6119, 294.575031 100, -5744, 29639.7679, 294.526897 101, -11443, 29634.9238, 294.478762 102, -12135, 29630.0797, 294.430627 103, -8318, 29625.2357, 294.382492 104, -3151, 29620.3916, 294.334357 105, -717, 29615.5476, 294.286222 106, -3079, 29610.7035, 294.238087 107, -8300, 29605.8594, 294.189953 108, -11478, 29601.0154, 294.141818 109, -8504, 29596.1713, 294.093683 110, 360, 29591.3273, 294.045548 111, 10258, 29586.4832, 293.997413 112, 15328, 29581.6391, 293.949278 113, 13199, 29576.7951, 293.901143 114, 6577, 29571.9510, 293.853009 115, 688, 29567.1070, 293.804874 116, -1025, 29562.2629, 293.756739 117, 796, 29557.4188, 293.708604 118, 2780, 29552.5748, 293.660469 119, 2143, 29547.7307, 293.612334 120, -1208, 29542.8867, 293.564199 121, -5325, 29538.0426, 293.516065 122, -8420, 29533.1985, 293.467930 123, -10228, 29528.3545, 293.419795 124, -11481, 29523.5104, 293.371660 125, -12513, 29518.6664, 293.323525 126, -12697, 29513.8223, 293.275390 127, -11183, 29508.9782, 293.227255 128, -7909, 29504.1342, 293.179121 129, -3722, 29499.2901, 293.130986 130, 400, 29494.4461, 293.082851 131, 3967, 29489.6020, 293.034716 132, 6804, 29484.7579, 292.986581 133, 8517, 29479.9139, 292.938446 134, 8546, 29475.0698, 292.890311 135, 6932, 29470.2258, 292.842177 136, 4814, 29465.3817, 292.794042 137, 3755, 29460.5376, 292.745907 138, 4282, 29455.6936, 292.697772 139, 5154, 29450.8495, 292.649637 140, 4349, 29446.0055, 292.601502 141, 1062, 29441.1614, 292.553368 142, -3228, 29436.3173, 292.505233 143, -5740, 29431.4733, 292.457098 144, -4584, 29426.6292, 292.408963 145, -113, 29421.7852, 292.360828 146, 5667, 29416.9411, 292.312693 147, 10769, 29412.0970, 292.264558 148, 14162, 29407.2530, 292.216424 149, 15274, 29402.4089, 292.168289 150, 13216, 29397.5649, 292.120154 151, 7235, 29392.7208, 292.072019 152, -1679, 29387.8767, 292.023884 153, -9935, 29383.0327, 291.975749 154, -12898, 29378.1886, 291.927614 155, -8218, 29373.3446, 291.879480 156, 1912, 29368.5005, 291.831345 157, 11885, 29363.6564, 291.783210 158, 16595, 29358.8124, 291.735075 159, 14902, 29353.9683, 291.686940 160, 9759, 29349.1243, 291.638805 161, 5150, 29344.2802, 291.590670 162, 2838, 29339.4361, 291.542536 163, 1741, 29334.5921, 291.494401 164, -4, 29329.7480, 291.446266 165, -2801, 29324.9040, 291.398131 166, -5463, 29320.0599, 291.349996 167, -6960, 29315.2158, 291.301861 168, -7797, 29310.3718, 291.253726 169, -9344, 29305.5277, 291.205592 170, -11898, 29300.6837, 291.157457 171, -13795, 29295.8396, 291.109322 172, -12840, 29290.9955, 291.061187 173, -8761, 29286.1515, 291.013052 174, -4119, 29281.3074, 290.964917 175, -2512, 29276.4634, 290.916782 176, -5578, 29271.6193, 290.868648 177, -11512, 29266.7752, 290.820513 178, -16398, 29261.9312, 290.772378 179, -17062, 29257.0871, 290.724243 180, -13005, 29252.2431, 290.676108 181, -6165, 29247.3990, 290.627973 182, 730, 29242.5549, 290.579838 183, 5598, 29237.7109, 290.531704 184, 7466, 29232.8668, 290.483569 185, 6451, 29228.0228, 290.435434 186, 3766, 29223.1787, 290.387299 187, 1497, 29218.3346, 290.339164 188, 1532, 29213.4906, 290.291029 189, 3982, 29208.6465, 290.242894 190, 6607, 29203.8025, 290.194760 191, 6390, 29198.9584, 290.146625 192, 2393, 29194.1143, 290.098490 193, -2724, 29189.2703, 290.050355 194, -4461, 29184.4262, 290.002220 195, -454, 29179.5822, 289.954085 196, 6869, 29174.7381, 289.905950 197, 11772, 29169.8940, 289.857816 198, 9975, 29165.0500, 289.809681 199, 2590, 29160.2059, 289.761546 200, -4475, 29155.3619, 289.713411 201, -5360, 29150.5178, 289.665276 202, 829, 29145.6737, 289.617141 203, 9320, 29140.8297, 289.569006 204, 13700, 29135.9856, 289.520872 205, 11031, 29131.1416, 289.472737 206, 3677, 29126.2975, 289.424602 207, -3294, 29121.4534, 289.376467 208, -6403, 29116.6094, 289.328332 209, -5935, 29111.7653, 289.280197 210, -4626, 29106.9213, 289.232062 211, -4736, 29102.0772, 289.183928 212, -6379, 29097.2331, 289.135793 213, -8185, 29092.3891, 289.087658 214, -9010, 29087.5450, 289.039523 215, -8770, 29082.7010, 288.991388 216, -7891, 29077.8569, 288.943253 217, -6437, 29073.0128, 288.895118 218, -4066, 29068.1688, 288.846984 219, -756, 29063.3247, 288.798849 220, 2725, 29058.4807, 288.750714 221, 5240, 29053.6366, 288.702579 222, 6133, 29048.7925, 288.654444 223, 5520, 29043.9485, 288.606309 224, 3796, 29039.1044, 288.558174 225, 1108, 29034.2604, 288.510040 226, -2432, 29029.4163, 288.461905 227, -6024, 29024.5722, 288.413770 228, -8027, 29019.7282, 288.365635 229, -7015, 29014.8841, 288.317500 230, -3277, 29010.0401, 288.269365 231, 795, 29005.1960, 288.221231 232, 2182, 29000.3519, 288.173096 233, -446, 28995.5079, 288.124961 234, -5565, 28990.6638, 288.076826 235, -9872, 28985.8198, 288.028691 236, -10724, 28980.9757, 287.980556 237, -7880, 28976.1316, 287.932421 238, -3223, 28971.2876, 287.884287 239, 1026, 28966.4435, 287.836152 240, 3842, 28961.5995, 287.788017 241, 5478, 28956.7554, 287.739882 242, 6409, 28951.9113, 287.691747 243, 6488, 28947.0673, 287.643612 244, 5200, 28942.2232, 287.595477 245, 2610, 28937.3792, 287.547343 246, -171, 28932.5351, 287.499208 247, -1627, 28927.6910, 287.451073 248, -1072, 28922.8470, 287.402938 249, 743, 28918.0029, 287.354803 250, 2255, 28913.1589, 287.306668 251, 2432, 28908.3148, 287.258533 252, 1609, 28903.4707, 287.210399 253, 1037, 28898.6267, 287.162264 254, 1559, 28893.7826, 287.114129 255, 2604, 28888.9386, 287.065994 256, 2483, 28884.0945, 287.017859 257, -144, 28879.2504, 286.969724 258, -4833, 28874.4064, 286.921589 259, -9221, 28869.5623, 286.873455 260, -10486, 28864.7183, 286.825320 261, -7409, 28859.8742, 286.777185 262, -1427, 28855.0301, 286.729050 263, 4166, 28850.1861, 286.680915 264, 6327, 28845.3420, 286.632780 265, 4112, 28840.4980, 286.584645 266, -1057, 28835.6539, 286.536511 267, -6651, 28830.8098, 286.488376 268, -10619, 28825.9658, 286.440241 269, -12089, 28821.1217, 286.392106 270, -11033, 28816.2777, 286.343971 271, -7769, 28811.4336, 286.295836 272, -3064, 28806.5895, 286.247701 273, 1449, 28801.7455, 286.199567 274, 3558, 28796.9014, 286.151432 275, 1866, 28792.0574, 286.103297 276, -2688, 28787.2133, 286.055162 277, -6889, 28782.3692, 286.007027 278, -7399, 28777.5252, 285.958892 279, -3484, 28772.6811, 285.910757 280, 2176, 28767.8371, 285.862623 281, 5625, 28762.9930, 285.814488 282, 5039, 28758.1489, 285.766353 283, 2296, 28753.3049, 285.718218 284, 1137, 28748.4608, 285.670083 285, 3506, 28743.6168, 285.621948 286, 7473, 28738.7727, 285.573813 287, 8810, 28733.9286, 285.525679 288, 4839, 28729.0846, 285.477544 289, -2997, 28724.2405, 285.429409 290, -10215, 28719.3965, 285.381274 291, -12989, 28714.5524, 285.333139 292, -11049, 28709.7083, 285.285004 293, -7273, 28704.8643, 285.236869 294, -4688, 28700.0202, 285.188735 295, -3907, 28695.1762, 285.140600 296, -3314, 28690.3321, 285.092465 297, -1427, 28685.4880, 285.044330 298, 1198, 28680.6440, 284.996195 299, 2482, 28675.7999, 284.948060 300, 1077, 28670.9559, 284.899925 301, -2030, 28666.1118, 284.851791 302, -4246, 28661.2677, 284.803656 303, -3718, 28656.4237, 284.755521 304, -990, 28651.5796, 284.707386 305, 1556, 28646.7356, 284.659251 306, 1895, 28641.8915, 284.611116 307, 128, 28637.0475, 284.562981 308, -1691, 28632.2034, 284.514847 309, -1371, 28627.3593, 284.466712 310, 1536, 28622.5153, 284.418577 311, 5265, 28617.6712, 284.370442 312, 6975, 28612.8272, 284.322307 313, 4618, 28607.9831, 284.274172 314, -1653, 28603.1390, 284.226038 315, -9312, 28598.2950, 284.177903 316, -14646, 28593.4509, 284.129768 317, -14743, 28588.6069, 284.081633 318, -9217, 28583.7628, 284.033498 319, -532, 28578.9187, 283.985363 320, 7481, 28574.0747, 283.937228 321, 12044, 28569.2306, 283.889094 322, 13027, 28564.3866, 283.840959 323, 12451, 28559.5425, 283.792824 324, 12296, 28554.6984, 283.744689 325, 12532, 28549.8544, 283.696554 326, 11113, 28545.0103, 283.648419 327, 5983, 28540.1663, 283.600284 328, -2726, 28535.3222, 283.552150 329, -12254, 28530.4781, 283.504015 330, -18929, 28525.6341, 283.455880 331, -20573, 28520.7900, 283.407745 332, -17725, 28515.9460, 283.359610 333, -12969, 28511.1019, 283.311475 334, -9210, 28506.2578, 283.263340 335, -8178, 28501.4138, 283.215206 336, -9854, 28496.5697, 283.167071 337, -12676, 28491.7257, 283.118936 338, -14265, 28486.8816, 283.070801 339, -12561, 28482.0375, 283.022666 340, -7141, 28477.1935, 282.974531 341, 111, 28472.3494, 282.926396 342, 5823, 28467.5054, 282.878262 343, 7338, 28462.6613, 282.830127 344, 4757, 28457.8172, 282.781992 345, 987, 28452.9732, 282.733857 346, -520, 28448.1291, 282.685722 347, 1422, 28443.2851, 282.637587 348, 4840, 28438.4410, 282.589452 349, 6420, 28433.5969, 282.541318 350, 4403, 28428.7529, 282.493183 351, -18, 28423.9088, 282.445048 352, -3858, 28419.0648, 282.396913 353, -4749, 28414.2207, 282.348778 354, -2430, 28409.3766, 282.300643 355, 1606, 28404.5326, 282.252508 356, 5373, 28399.6885, 282.204374 357, 7188, 28394.8445, 282.156239 358, 5826, 28390.0004, 282.108104 359, 854, 28385.1563, 282.059969 360, -6487, 28380.3123, 282.011834 361, -12922, 28375.4682, 281.963699 362, -14618, 28370.6242, 281.915564 363, -10069, 28365.7801, 281.867430 364, -1918, 28360.9360, 281.819295 365, 4538, 28356.0920, 281.771160 366, 5526, 28351.2479, 281.723025 367, 2077, 28346.4039, 281.674890 368, -832, 28341.5598, 281.626755 369, 1194, 28336.7157, 281.578620 370, 7881, 28331.8717, 281.530486 371, 14514, 28327.0276, 281.482351 372, 16243, 28322.1836, 281.434216 373, 12301, 28317.3395, 281.386081 374, 6144, 28312.4954, 281.337946 375, 1751, 28307.6514, 281.289811 376, 114, 28302.8073, 281.241676 377, -579, 28297.9633, 281.193542 378, -1756, 28293.1192, 281.145407 379, -2260, 28288.2751, 281.097272 380, 164, 28283.4311, 281.049137 381, 5395, 28278.5870, 281.001002 382, 9766, 28273.7430, 280.952867 383, 9224, 28268.8989, 280.904732 384, 3854, 28264.0548, 280.856598 385, -1267, 28259.2108, 280.808463 386, -534, 28254.3667, 280.760328 387, 6435, 28249.5227, 280.712193 388, 13683, 28244.6786, 280.664058 389, 14112, 28239.8345, 280.615923 390, 6281, 28234.9905, 280.567788 391, -3832, 28230.1464, 280.519654 392, -8048, 28225.3024, 280.471519 393, -3308, 28220.4583, 280.423384 394, 5800, 28215.6142, 280.375249 395, 11486, 28210.7702, 280.327114 396, 9612, 28205.9261, 280.278979 397, 2458, 28201.0821, 280.230845 398, -4584, 28196.2380, 280.182710 399, -8292, 28191.3939, 280.134575 400, -9397, 28186.5499, 280.086440 401, -9784, 28181.7058, 280.038305 402, -9116, 28176.8618, 279.990170 403, -5174, 28172.0177, 279.942035 404, 2472, 28167.1736, 279.893901 405, 10064, 28162.3296, 279.845766 406, 12024, 28157.4855, 279.797631 407, 6280, 28152.6415, 279.749496 408, -3049, 28147.7974, 279.701361 409, -8930, 28142.9533, 279.653226 410, -7851, 28138.1093, 279.605091 411, -2995, 28133.2652, 279.556957 412, -790, 28128.4212, 279.508822 413, -4154, 28123.5771, 279.460687 414, -9321, 28118.7330, 279.412552 415, -9639, 28113.8890, 279.364417 416, -2591, 28109.0449, 279.316282 417, 7086, 28104.2009, 279.268147 418, 11531, 28099.3568, 279.220013 419, 7210, 28094.5127, 279.171878 420, -1657, 28089.6687, 279.123743 421, -7051, 28084.8246, 279.075608 422, -4602, 28079.9806, 279.027473 423, 2703, 28075.1365, 278.979338 424, 7932, 28070.2924, 278.931203 425, 7083, 28065.4484, 278.883069 426, 2599, 28060.6043, 278.834934 427, 289, 28055.7603, 278.786799 428, 3061, 28050.9162, 278.738664 429, 7809, 28046.0721, 278.690529 430, 8473, 28041.2281, 278.642394 431, 2123, 28036.3840, 278.594259 432, -7835, 28031.5400, 278.546125 433, -14259, 28026.6959, 278.497990 434, -12123, 28021.8518, 278.449855 435, -2354, 28017.0078, 278.401720 436, 9295, 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